Spectrometers
Publication details: please check below which grants need to be acknowledged when publishing results obtained with the help of NMR (instrument specific). The corresponding GISMO codes also need to be mentioned when submitting your publications to the academic biblio of the UGent.
The spectrometers listed below are all managed by the NMR expertise center. In general there are two categories to be discerned:
Open access infrastructure
These spectrometers operate 24/7 in a semi-automated environment and are available for researchers to measure in an independent manner following a short training organized by Emile Ottoy (CTO).
- 300MHz (Phobos)
- 400MHZ (Deimos)
Research infrastructure
This infrastructure is accessible to dedicated researchers only, following a clear and adequate motivation illustrating the research needs. The researcher in questions needs to follow an in-depth training before access is allowed.
- 500MHz (Nestor)
- 500MHz (Hercules)
- 700MHz (Hera)
300MHz Avance I (Bruker) - Phobos
Technical description
• 5mm dual channel probe head - 1H and Broadband (BBO-type)
• Running Topspin 2.1 in ICONNMR environment
• Fully automated SampleXpress sample changer for 60 samples
• Ultrashield type magnet
400MHz Avance NEO (Bruker) - Deimos
Technical description
• 5mm dual channel N2 cryoprobe - 1H and Broadband (Prodigy BBO-type)
• 5mm dual channel probe head - 1H and Broadband (BBO-type)
• Prodigy Cryoplatform
• Running Topspin 4.3 in ICONNMR environment
• Fully automated Sample Xpress sample changer for 60 samples
• Ultrashield type magnet
The 400MHz is funded thanks to the following grants:
- Upgrade of the old room temperature BBO probe to a Prodigy cryoprobe: FWO I006920N
(GISMO code 319309020) - Renewal of the spectrometer console to Avance NEO: Ghent University BOF.BAS.2022.0023.01
(GISMO code BOF/BAS/2022/105)
500MHz Avance III (Bruker) - Hercules
Technical description
• 4mm dual channel HR-MAS iProbe - 1H and 13C (soft matter)
• 4mm dual channel CPMAS iProbe - 1H and Broadband (solid state)
• 5mm dual channel probe head - 1H and Broadband (BBI-type, liquid state)
• 5mm dual channel High Gradient probe
• MAS III Pneumatic Unit
• Running Topspin 3.6
• Automated sample changer for 10 MAS 4mm rotors
• Ascend type magnet
The 500MHz is funded thanks to the following grants:
- Spectrometer + magnet and accessories, including BBI and high-gradient diffusion probe: Hercules foundation AUGE/09/2006
(GISMO code 19201210) - Solid state (CP-MAS) and HR-MAS conversion: FWO I006920N
(GISMO code 319309020)
500MHz Avance III HD (Bruker) - Nestor
Technical description
• 5mm tripple channel probe head - 1H 13C 19F (TXO type)
• Running Topspin 3.6
• Fully automated bacs sample changer for 60 samples
• Oxford type magnet
The 500MHz is funded thanks to the following grants:
- Installation of the TXO 1H/19F/13C room temperature probe: FWO G011015N
- Renewal of the spectrometer console to Avance III HD: Ghent University BOF.BAS.20200019.01
(GISMO code 01B07520)
700MHz Avance II (Bruker) - Hera
Technical description
• 5mm triple channel N2 cryoprobe - 1H/19F 13C 15N (Prodigy TCI-type)
• 5mm triple channel probe head - 1H 13C 15N (TXI-type)
• 1mm triple channel probe head - 1H 13C 15N (TXI-type)
• Prodigy Cryoplatform
• Running Topspin 3.1
• Fully automated bacs sample changer for 60 samples
• Ultrashield + type magnet
The 700MHz is funded thanks to the following grants:
- Spectrometer + magnet and accessories: FFEU-ZWAP (2003)
- Upgrade of the old room temperature TXI probe to a Prodigy cryoprobe: Hercules foundation AUGE/15/2012
(GISMO code 319202316) - Upgrade of the Avance II to an Avance NEO console: FWO Infrastructure I009324N (2024)